5MA9
GFP-binding DARPin fusion gc_R11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-19 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 |
Unit cell lengths | 81.880, 89.890, 90.040 |
Unit cell angles | 95.84, 116.53, 92.35 |
Refinement procedure
Resolution | 44.682 - 1.570 |
R-factor | 0.1606 |
Rwork | 0.158 |
R-free | 0.20320 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.929 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.682 | 1.610 |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.046 | 0.569 |
Number of reflections | 302440 | |
<I/σ(I)> | 14.03 | 2.6 |
Completeness [%] | 95.2 | 94.4 |
Redundancy | 3.4 | 3.62 |
CC(1/2) | 0.990 | 0.754 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M TRIS pH 8.5, 30% w/v PEG 4000, 0.2 M LiSO4 |