5MA3
GFP-binding DARPin fusion gc_R11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-18 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.850, 90.610, 60.920 |
Unit cell angles | 90.00, 103.42, 90.00 |
Refinement procedure
Resolution | 48.979 - 1.700 |
R-factor | 0.1627 |
Rwork | 0.161 |
R-free | 0.19160 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.851 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.979 | 1.740 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.105 | 3.440 |
Number of reflections | 67771 | |
<I/σ(I)> | 10.47 | 0.98 |
Completeness [%] | 97.6 | 98.6 |
Redundancy | 6.7 | 6.9 |
CC(1/2) | 0.997 | 0.561 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M Sodium Acetate, 0.1 M Sodium Cacodylate pH 6.5, 30% w/v PEG 8000 |