5M9T
Human angiogenin ALS variant H114R
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-11 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9763 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 81.426, 81.426, 85.985 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 70.500 - 2.200 |
R-factor | 0.18556 |
Rwork | 0.182 |
R-free | 0.23596 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ang |
RMSD bond length | 0.011 |
RMSD bond angle | 1.598 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.500 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 16435 | |
<I/σ(I)> | 12.1 | 1.8 |
Completeness [%] | 95.8 | 75.9 |
Redundancy | 9.5 | 3.6 |
CC(1/2) | 0.994 | 0.681 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 289 | 0.01 M Na borate 1.1 M Na citrate |