5M9E
Interactions between the Mal3 EB1-like domain and Dis1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2016-05-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 93.305, 93.305, 196.545 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 80.800 - 2.830 |
R-factor | 0.2691 |
Rwork | 0.266 |
R-free | 0.32450 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5m97 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.524 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.800 | 2.931 |
High resolution limit [Å] | 2.830 | 2.830 |
Rmerge | 0.177 | 2.937 |
Number of reflections | 12733 | |
<I/σ(I)> | 9.13 | 1.3 |
Completeness [%] | 97.0 | 100 |
Redundancy | 18.3 | 19 |
CC(1/2) | 0.580 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.2 M MgCl2, 0.1 M HEPES pH 7, 20% PEG 6K |