5M6G
Crystal structure Glucan 1,4-beta-glucosidase from Saccharopolyspora erythraea
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.033121 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.292, 75.717, 113.893 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.511 - 1.829 |
R-factor | 0.173 |
Rwork | 0.172 |
R-free | 0.20350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ieq |
RMSD bond length | 0.006 |
RMSD bond angle | 0.819 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.829 |
Number of reflections | 47457 |
<I/σ(I)> | 11.27 |
Completeness [%] | 95.1 |
Redundancy | 3.35 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 15% PEG 20K, 100mM MES Sodium Salt, 80 mM Mangan II Chloride |