5M60
Chaetomium thermophilum beta-1-3-glucanase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.661, 83.535, 65.171 |
Unit cell angles | 90.00, 93.10, 90.00 |
Refinement procedure
Resolution | 44.291 - 1.500 |
R-factor | 0.1582 |
Rwork | 0.157 |
R-free | 0.18160 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 0.865 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.300 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.009 | 0.765 |
Number of reflections | 106298 | |
<I/σ(I)> | 10.3 | 1.8 |
Completeness [%] | 99.8 | 96.4 |
Redundancy | 4.9 | 5.1 |
CC(1/2) | 0.998 | 0.582 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 289 | 1.8 M Na/K phosphate |