5M3X
Crystal structure of human angiotensin I-deleted angiotensinogen
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-17 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 86.300, 41.040, 129.950 |
Unit cell angles | 90.00, 107.82, 90.00 |
Refinement procedure
Resolution | 43.440 - 2.630 |
R-factor | 0.2439 |
Rwork | 0.242 |
R-free | 0.28230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wxw |
RMSD bond length | 0.002 |
RMSD bond angle | 0.559 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.440 | 2.700 |
High resolution limit [Å] | 2.630 | 2.630 |
Rmerge | 0.139 | 0.801 |
Number of reflections | 26239 | |
<I/σ(I)> | 6.9 | 1.3 |
Completeness [%] | 99.3 | 99.3 |
Redundancy | 3.3 | 3.3 |
CC(1/2) | 0.534 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 1.7M Ammonium Sulfate, 0.1M Citric Acid, pH3.6 |