5M2N
Crystal Structure of Elongator subunit Elp2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-17 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.978980 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 79.690, 79.690, 532.150 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.894 - 2.812 |
R-factor | 0.2014 |
Rwork | 0.200 |
R-free | 0.23650 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.557 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | autoSHARP |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.890 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.143 | 0.819 |
Number of reflections | 45798 | |
<I/σ(I)> | 14.4 | 2.58 |
Completeness [%] | 99.6 | 95.7 |
Redundancy | 9.3 | 7.2 |
CC(1/2) | 0.990 | 0.680 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 100 mM Tris pH 7.5; 10% PEG 6K; 1750 mM NaCl |