5M24
RARg mutant-S371E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-06-21 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9334 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 59.871, 59.871, 157.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.690 |
R-factor | 0.19646 |
Rwork | 0.194 |
R-free | 0.23361 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3lbd |
RMSD bond length | 0.007 |
RMSD bond angle | 1.118 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.720 |
High resolution limit [Å] | 1.690 | 1.690 |
Rmerge | 0.044 | |
Number of reflections | 32495 | |
<I/σ(I)> | 70.17 | 11.81 |
Completeness [%] | 100.0 | 99 |
Redundancy | 13.4 | 12.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 290 | 0.2 M Calcium Chloride, 0.1 M, Tris HCl pH 7.5, 14% Peg 6K |