5LY5
Arcadin-1 from Pyrobaculum calidifontis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97949 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 84.051, 84.051, 61.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.20961 |
Rwork | 0.208 |
R-free | 0.23032 |
Structure solution method | SIRAS |
RMSD bond length | 0.020 |
RMSD bond angle | 2.121 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.065 | 1.348 |
Number of reflections | 9095 | |
<I/σ(I)> | 26.6 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 19 | 19.7 |
CC(1/2) | 1.000 | 0.903 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 7.2 % MPD (v/v), 14 mM MgCl2, 50 mM sodium cacodylate pH 6.0 |