5LVU
XiaF (apo) from Streptomyces sp.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-10 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 166.540, 166.540, 98.970 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.600 |
R-factor | 0.18398 |
Rwork | 0.182 |
R-free | 0.21759 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jbr |
RMSD bond length | 0.004 |
RMSD bond angle | 0.788 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.085 | 0.563 |
Number of reflections | 25318 | |
<I/σ(I)> | 16.5 | 4.3 |
Completeness [%] | 99.6 | 99.7 |
Redundancy | 10.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 1.6 M ammonium sulfate, 0.1 M HEPES, 0.1 M sodium chloride |