5LTD
Phosphate-bound Pichia angusta Atg18
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-16 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 58.242, 58.253, 62.250 |
Unit cell angles | 83.73, 80.85, 86.77 |
Refinement procedure
Resolution | 45.000 - 2.500 |
Rwork | 0.221 |
R-free | 0.26500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ltg |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | |
High resolution limit [Å] | 2.500 | |
Rmerge | 0.133 | 0.645 |
Number of reflections | 27376 | |
<I/σ(I)> | 12.8 | |
Completeness [%] | 98.3 | 96.5 |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 20 % (w/V) PEG 8000, 0.2 M NaCl, 0.1 M sodium phosphate dibasic-citric acid pH 4.2 |