5LSF
Sacbrood honeybee virus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-03-28 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97857 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 487.850, 360.970, 338.160 |
| Unit cell angles | 90.00, 133.07, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.100 |
| Rwork | 0.194 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1b35 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.440 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.140 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.135 | 0.639 |
| Number of reflections | 1572113 | |
| <I/σ(I)> | 6.6 | 1 |
| Completeness [%] | 64.0 | 21.5 |
| Redundancy | 3.1 | 1.4 |
| CC(1/2) | 0.977 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277.15 | PEG4000, isopropanol, magnesium chloride, MES |
