5LQ9
CRYSTAL STRUCTURE OF HSP90 IN COMPLEX WITH SAR200323.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-11-28 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 66.738, 90.028, 98.555 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.460 - 1.900 |
Rwork | 0.196 |
R-free | 0.23600 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.900 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.489 | |
Number of reflections | 23773 | |
<I/σ(I)> | 28.1 | 4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.1 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 1.0 to 1.4M Sodium Citrate |