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5LPV

Crystal structure of the BRI1 kinase domain (865-1160) in complex with AMPPNP and Mn from Arabidopsis thaliana

Replaces:  4OA9
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-08-19
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.000040
Spacegroup nameP 62
Unit cell lengths115.630, 115.630, 49.640
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution44.475 - 2.700
R-factor0.1929
Rwork0.191
R-free0.23280
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3uim
RMSD bond length0.002
RMSD bond angle0.597
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.4802.860
High resolution limit [Å]2.7002.700
Number of reflections10619
<I/σ(I)>12.35
Completeness [%]97.997.9
Redundancy12.0911.98
CC(1/2)0.851
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.529828% PEG 20K/MME 550 morpheus mix, 0.12 M eth glycol mix, 0.1 M Hepes pH 6.5

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