5LNU
Crystal structure of Arabidopsis thaliana Pdx1-I320 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.91730 |
Spacegroup name | H 3 |
Unit cell lengths | 178.117, 178.117, 115.963 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.346 - 1.730 |
R-factor | 0.1638 |
Rwork | 0.162 |
R-free | 0.19120 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 0.813 |
Data scaling software | Aimless (0.5.17) |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 52.200 | 52.200 | 1.760 |
High resolution limit [Å] | 1.730 | 9.480 | 1.730 |
Rmerge | 0.054 | 0.021 | 0.445 |
Rmeas | 0.066 | 0.025 | 0.548 |
Rpim | 0.037 | 0.013 | 0.316 |
Total number of observations | 408071 | 2821 | 20789 |
Number of reflections | 141425 | ||
<I/σ(I)> | 9.3 | 29.9 | 1.9 |
Completeness [%] | 98.1 | 99.4 | 99.7 |
Redundancy | 2.9 | 3.2 | 2.9 |
CC(1/2) | 0.997 | 0.999 | 0.841 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 0.1 M Tris pH8.5, 0.13 M sodium acetate pH5.5, 12.25%(w/v) PEG4000 |