5LN1
STRUCTURE OF UBIQUITYLATED-RPN10 FROM YEAST;
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9393 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 107.290, 49.700, 81.330 |
Unit cell angles | 90.00, 130.55, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.800 | 3.310 |
High resolution limit [Å] | 3.140 | 3.140 |
Rmerge | 0.084 | 0.225 |
Number of reflections | 5824 | |
<I/σ(I)> | 10.2 | 5.1 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 3.2 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION, RECRYSTALLIZATION | 6.5 | 292 | 12% (W/V) PEG 20000, 0.1M MES PH 6.5, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 292K |