5LN0
Low dose Thaumatin - 760-800 ms.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 296 |
Detector technology | PIXEL |
Collection date | 2015-10-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.96863 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 58.450, 58.450, 151.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.940 - 1.950 |
R-factor | 0.184 |
Rwork | 0.182 |
R-free | 0.22390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lr2 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.717 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.950 | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.137 | 0.529 |
Number of reflections | 18238 | |
<I/σ(I)> | 5.7 | 1.8 |
Completeness [%] | 91.3 | 92.1 |
Redundancy | 3.1 | 3.1 |
CC(1/2) | 0.985 | 0.711 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 1.3 M sodium tartrate, 50 mM Bis-Tris pH 6.8 |