5LMW
Llama nanobody PorM_02
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-09-09 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.8729 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 65.680, 65.680, 88.802 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.580 - 1.500 |
R-factor | 0.188 |
Rwork | 0.188 |
R-free | 0.19600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4y7m |
RMSD bond length | 0.010 |
RMSD bond angle | 0.980 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.440 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.047 | |
Number of reflections | 31805 | |
<I/σ(I)> | 22 | 1.7 |
Completeness [%] | 99.9 | 99.4 |
Redundancy | 6.8 | 6.5 |
CC(1/2) | 0.627 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293.15 | Tri-sodium Citrate PEG 3000 |