5LKM
RadA bound to dTDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 99.400, 169.900, 187.420 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.210 - 3.500 |
R-factor | 0.18497 |
Rwork | 0.183 |
R-free | 0.22398 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5lko |
RMSD bond length | 0.014 |
RMSD bond angle | 1.823 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.8.0124) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.210 | |
High resolution limit [Å] | 3.500 | |
Rmerge | 0.184 | 1.071 |
Rmeas | 0.185 | 1.079 |
Number of reflections | 20413 | |
<I/σ(I)> | 22.76 | |
Completeness [%] | 100.0 | |
Redundancy | 66.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | 200 mM MgF 100 mM HEPES pH8 |