5LF9
Crystal structure of human NUDT22
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-24 |
Detector | DECTRIS PILATUS3 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.810, 52.114, 101.783 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.390 - 1.450 |
R-factor | 0.17283 |
Rwork | 0.171 |
R-free | 0.20705 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.656 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.390 | 1.530 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.084 | 1.005 |
Number of reflections | 47830 | |
<I/σ(I)> | 15 | 2.6 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 13 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 15% HighPEG, 0.1 M hepes pH 7.5, 0.1 M NaKPO, 10% EDO |