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5LEE

Crystal structure of DARPin-DARPin rigid fusion, variant DDD_D12_12_D12_12_D12

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-05-06
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.00
Spacegroup nameP 32 2 1
Unit cell lengths69.260, 69.260, 230.490
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution47.279 - 2.401
R-factor0.2506
Rwork0.249
R-free0.27400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1SVX chain A
RMSD bond length0.002
RMSD bond angle0.426
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX ((dev_2400))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]47.2792.487
High resolution limit [Å]2.4012.401
Rmerge0.0920.230
Number of reflections25927
<I/σ(I)>18.38
Completeness [%]96.7
Redundancy19.4
CC(1/2)0.999
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.5293PEG 3350 20% w/v, Sodium citrate 0.2 M, Bis-Tris propane 0.1 M, pH 8.5

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