5LE0
MICAL1 Cterminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.978870 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 52.780, 52.780, 157.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.800 - 3.300 |
R-factor | 0.2725 |
Rwork | 0.271 |
R-free | 0.30630 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.597 |
Data reduction software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.800 | 3.418 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.043 | 0.317 |
Number of reflections | 3734 | |
<I/σ(I)> | 26.56 | |
Completeness [%] | 99.6 | |
Redundancy | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 290 | EG |