5LDY
Structure of Yersinia pseudotuberculosis InvD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-14 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0000 |
Spacegroup name | P 43 |
Unit cell lengths | 58.900, 58.900, 274.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.701 - 2.600 |
R-factor | 0.2331 |
Rwork | 0.230 |
R-free | 0.25300 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.470 |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.701 | 2.700 | |
High resolution limit [Å] | 2.600 | 10.000 | 2.600 |
Rmerge | 0.063 | 0.024 | 0.416 |
Number of reflections | 28540 | ||
<I/σ(I)> | 26.62 | 65.41 | 5.86 |
Completeness [%] | 99.9 | 99 | 99.9 |
Redundancy | 11.3 | ||
CC(1/2) | 0.999 | 1.000 | 0.957 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 1.9 M ammonium dihydrogen phosphate; 0.1 M TRIS-HCl pH 8.0 |