5LDV
Crystal Structures of MOMP from Campylobacter jejuni
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-06-27 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.06733 |
Spacegroup name | P 63 |
Unit cell lengths | 90.630, 90.630, 104.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.240 - 2.100 |
R-factor | 0.19497 |
Rwork | 0.193 |
R-free | 0.22241 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.397 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.240 | 2.175 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.060 | |
Number of reflections | 28313 | |
<I/σ(I)> | 29.89 | |
Completeness [%] | 99.5 | |
Redundancy | 13.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.25 | 295.15 | 0.05M sodium citrate, 35% (v/v) Peg 400, 0.07 M potassium chloride |