5LDN

A viral capsid:antibody complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E SUPERBRIGHT
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2012-12-10
Detector	RIGAKU RAXIS II
Wavelength(s)	0.987
Spacegroup name	P 63
Unit cell lengths	156.999, 156.999, 144.891
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	78.500 - 2.700
R-factor	0.1673
Rwork	0.164
R-free	0.22290
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3tg7
RMSD bond length	0.014
RMSD bond angle	1.669
Data scaling software	SCALA (3.3.20)
Refinement software	REFMAC (5.8.0151)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	135.931	10.000	2.850
High resolution limit [Å]	2.700	8.000	2.700
Rmerge		0.060	0.964
Rmeas	0.176
Rpim	0.058
Total number of observations	520799
Number of reflections	55555
<I/σ(I)>	11.8	4.4	0.7
Completeness [%]	100.0	99.9	100
Redundancy	9.4	9.2	9.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277	PEG 4000, sodium chloride,