5LDI
Crystal structure of E.coli LigT in apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-05-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.033 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.390, 88.320, 73.840 |
Unit cell angles | 90.00, 115.01, 90.00 |
Refinement procedure
Resolution | 36.604 - 2.100 |
R-factor | 0.1799 |
Rwork | 0.177 |
R-free | 0.22670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDBid:1iuh |
RMSD bond length | 0.004 |
RMSD bond angle | 0.981 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.076 | 0.918 |
Number of reflections | 43063 | |
<I/σ(I)> | 11.93 | 1.3 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 3.81 | 3.83 |
CC(1/2) | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.1 M Tris-HCl pH 7.5, 0.2 M MgCl2, 14% (w/v) PEG 8000 |