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5L9A

L-threonine dehydrogenase from trypanosoma brucei.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-2
Synchrotron siteESRF
BeamlineID23-2
Temperature [K]100
Detector technologyCCD
Collection date2009-09-21
DetectorMARRESEARCH
Wavelength(s)0.8726
Spacegroup nameP 1
Unit cell lengths46.985, 57.722, 70.074
Unit cell angles72.46, 70.38, 73.20
Refinement procedure
Resolution46.820 - 1.450
R-factor0.10254
Rwork0.100
R-free0.15643
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2yy7
RMSD bond length0.021
RMSD bond angle2.070
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0135)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]53.8201.530
High resolution limit [Å]1.4501.450
Rmerge0.0890.398
Number of reflections109054
<I/σ(I)>10.42.7
Completeness [%]95.082.1
Redundancy3.82.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52930.1 M HEPES pH 7.5, 20 % w/v PEG 10K, TDH 2.0 mg/ml

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