5L80
Structure of Exuperantia EXO-like and SAM-like domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.540, 66.590, 81.330 |
Unit cell angles | 90.00, 113.64, 90.00 |
Refinement procedure
Resolution | 47.336 - 2.800 |
R-factor | 0.2535 |
Rwork | 0.252 |
R-free | 0.27650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5l7z |
RMSD bond length | 0.003 |
RMSD bond angle | 0.658 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.078 | 1.045 |
Number of reflections | 19360 | |
<I/σ(I)> | 19.4 | 2.2 |
Completeness [%] | 99.5 | 99.2 |
Redundancy | 6.7 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | Sodium Malonate, PEG 1000, MES |