5L7Z

Structure of Exuperantia EXO-like domain

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X10SA
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-06-21
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.980, 1.040, 1.0
Spacegroup name	P 61 2 2
Unit cell lengths	79.890, 79.890, 237.280
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	45.034 - 2.370
R-factor	0.2052
Rwork	0.204
R-free	0.22360
Structure solution method	MAD
RMSD bond length	0.002
RMSD bond angle	0.468
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHELXCD
Refinement software	PHENIX ((1.10.1_2155))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.470
High resolution limit [Å]	2.370	2.370
Rmerge	0.085	0.972
Number of reflections	19097
<I/σ(I)>	23.98
Completeness [%]	100.0	100
Redundancy	19

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	277	MPD, MES