5L7G
MCR IN COMPLEX WITH ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.976 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.635, 77.704, 78.314 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.320 - 2.010 |
R-factor | 0.209 |
Rwork | 0.207 |
R-free | 0.24340 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.000 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Refinement software | BUSTER (2.11.6 PACIOREK) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.630 |
High resolution limit [Å] | 2.010 |
Rmerge | 0.145 |
Number of reflections | 20315 |
<I/σ(I)> | 11.4 |
Completeness [%] | 99.6 |
Redundancy | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 293 | 0.9 M AMS 0.1 M CHES pH 9.5 +10% Morpheus C9 |