5L74
Plexin A2 extracellular segment domains 4-5 (PSI2-IPT2), resolution 1.36 Angstrom
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2012-12-08 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1.0163 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 107.710, 44.560, 33.010 |
Unit cell angles | 90.00, 104.70, 90.00 |
Refinement procedure
Resolution | 52.092 - 1.360 |
R-factor | 0.1759 |
Rwork | 0.174 |
R-free | 0.20250 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.298 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2283: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 52.100 |
High resolution limit [Å] | 1.360 |
Number of reflections | 27859 |
<I/σ(I)> | 17 |
Completeness [%] | 85.6 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.5 | 25% (w/v) polyethylene glycol 3,350 and 100 mM BIS-TRIS pH 5.5 |