5L6Y
il13 in complex with tralokinumab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-16 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9749 |
Spacegroup name | P 1 |
Unit cell lengths | 50.998, 53.195, 62.050 |
Unit cell angles | 107.91, 101.42, 96.94 |
Refinement procedure
Resolution | 49.650 - 1.990 |
R-factor | 0.19 |
Rwork | 0.189 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | in-house model |
RMSD bond length | 0.022 |
RMSD bond angle | 1.180 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.6) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.650 | 2.100 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.130 | 0.320 |
Number of reflections | 39821 | |
<I/σ(I)> | 11.7 | 2.1 |
Completeness [%] | 97.7 | 93.4 |
Redundancy | 10.5 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | sodium formate |