5L5N
Plexin A4 full extracellular region, domains 1 to 7 modeled, data to 8.5 angstrom, spacegroup P4(3)22
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9763 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 189.480, 189.480, 252.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 70.367 - 8.502 |
R-factor | 0.4017 |
Rwork | 0.401 |
R-free | 0.41170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5l56 |
RMSD bond length | 0.019 |
RMSD bond angle | 2.473 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.000 | |
High resolution limit [Å] | 8.500 | 8.500 |
Rmerge | 0.330 | 1.170 |
Number of reflections | 4374 | |
<I/σ(I)> | 4.2 | |
Completeness [%] | 99.7 | |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293.5 | 1.5 lithium sulfate, 100 mM TRIS, pH 8.5 |