5L5L
Plexin A4 full extracellular region, domains 1 to 8 modeled, data to 8 angstrom, spacegroup P2(1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-12-13 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9763 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 142.180, 241.000, 144.070 |
Unit cell angles | 90.00, 99.83, 90.00 |
Refinement procedure
Resolution | 47.741 - 8.001 |
R-factor | 0.3494 |
Rwork | 0.349 |
R-free | 0.34920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5l56 |
RMSD bond length | 0.019 |
RMSD bond angle | 2.464 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 | |
High resolution limit [Å] | 8.000 | 8.000 |
Rmerge | 0.158 | 0.764 |
Number of reflections | 10061 | |
<I/σ(I)> | 9 | |
Completeness [%] | 99.5 | |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293.5 | 0.5 M sodium succinate, 100 mM bis-TRIS propane, pH 7.0 |