5L5C
Plexin A1 full extracellular region, domains 1 to 10, to 6 angstrom, spacegroup P4(3)2(1)2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-05-29 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.9173 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 198.150, 198.150, 228.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 119.503 - 6.000 |
R-factor | 0.3052 |
Rwork | 0.305 |
R-free | 0.31610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5l56 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.242 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 119.503 | |
High resolution limit [Å] | 6.000 | 6.000 |
Rmerge | 0.710 | 1.240 |
Number of reflections | 11641 | |
<I/σ(I)> | 9.7 | |
Completeness [%] | 98.8 | |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293.5 | 6% (w/v) PEG 4k, 5 mM tricine, pH 8.5 |