5L59
Plexin A1 full extracellular region, domains 1 to 10, to 6 angstrom, spacegroup P2(1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-04-20 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0719 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 139.990, 196.450, 144.940 |
Unit cell angles | 90.00, 94.57, 90.00 |
Refinement procedure
Resolution | 58.218 - 6.000 |
R-factor | 0.275 |
Rwork | 0.274 |
R-free | 0.29950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5l56 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.250 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 58.218 |
High resolution limit [Å] | 6.000 |
Number of reflections | 19391 |
<I/σ(I)> | 6.8 |
Completeness [%] | 99.7 |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293.5 | 15% (v/v) propanol, 20 mM magnesium chloride 50 mM MES, pH 6.0 |