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5L32

Crystal structure of the Zn-RIDC1 complex bearing six interfacial disulfide bonds

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL14-1
Synchrotron siteSSRL
BeamlineBL14-1
Temperature [K]100
Detector technologyCCD
Collection date2013-07-16
DetectorMARMOSAIC 325 mm CCD
Wavelength(s)0.98
Spacegroup nameP 1 21 1
Unit cell lengths48.060, 62.533, 72.437
Unit cell angles90.00, 99.01, 90.00
Refinement procedure
Resolution37.810 - 2.100
R-factor0.21563
Rwork0.214
R-free0.24972
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3hnj
RMSD bond length0.018
RMSD bond angle1.576
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0103)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]37.8102.210
High resolution limit [Å]2.1002.100
Rmerge0.0490.463
Number of reflections24815
<I/σ(I)>153
Completeness [%]99.599.3
Redundancy3.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.42940.2 M magnesium chloride, 0.1 M Bis-Tris (pH 6.5), 35% PEG 400

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