5KZX
Crystal structure of human GAA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL14-1 |
Synchrotron site | SSRL |
Beamline | BL14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-07 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.18076 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 97.110, 102.590, 128.550 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 80.310 - 2.000 |
R-factor | 0.156 |
Rwork | 0.154 |
R-free | 0.18500 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5KZR |
RMSD bond length | 0.010 |
RMSD bond angle | 1.469 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless (0.5.12) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.310 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.091 | 0.363 |
Number of reflections | 90718 | |
<I/σ(I)> | 12.9 | |
Completeness [%] | 89.2 | 47.8 |
Redundancy | 7.3 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.1 sodium HEPES, 2% (v/v) PEG 400, 2M ammonium sulfate |