5KXN
Hen Egg White Lysozyme at 100K, Data set 4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL14-1 |
Synchrotron site | SSRL |
Beamline | BL14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-07-19 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.21549 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.311, 77.311, 37.212 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.655 - 1.198 |
R-factor | 0.1601 |
Rwork | 0.159 |
R-free | 0.17780 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 2blx |
Data reduction software | XDS |
Data scaling software | SCALA (3.3.20) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 38.672 | 38.672 | 1.260 |
High resolution limit [Å] | 1.198 | 3.790 | 1.200 |
Rmerge | 0.030 | 0.240 | |
Rmeas | 0.035 | 0.033 | 0.264 |
Rpim | 0.014 | 0.014 | 0.108 |
Total number of observations | 238514 | 7499 | 29227 |
Number of reflections | 35957 | ||
<I/σ(I)> | 32.8 | 68.5 | 6.8 |
Completeness [%] | 99.6 | 99.2 | 97.9 |
Redundancy | 6.6 | 5.9 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 291 | CRYSTALS WERE GROWN BY MIXING EQUAL VOLUMES OF WELL SOLUTION (1.0 M SODIUM CHLORIDE, 50 MM SODIUM ACETATE PH 4.5) AND PROTEIN (40-60 MG/ML) |