5KWR
Crystal structure of rat Cerebellin-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2015-11-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.03321 |
Spacegroup name | P 6 |
Unit cell lengths | 82.740, 82.740, 50.370 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.370 - 1.795 |
R-factor | 0.1629 |
Rwork | 0.160 |
R-free | 0.18880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4oum |
RMSD bond length | 0.005 |
RMSD bond angle | 0.740 |
Data reduction software | XDS (Version Oct 15, 2015) |
Data scaling software | XDS (Version Oct 15, 2015) |
Phasing software | PHASER (2.6.0) |
Refinement software | PHENIX ((dev_2471: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.840 |
High resolution limit [Å] | 1.795 | 1.800 |
Rmerge | 0.040 | 0.644 |
Number of reflections | 18152 | |
<I/σ(I)> | 22.5 | 1.74 |
Completeness [%] | 98.2 | 83.8 |
Redundancy | 6.46 | 3.15 |
CC(1/2) | 1.000 | 0.729 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 294 | 0.1 M Tris pH 7.5, 3 M Sodium formate. Grown in the presence of Neurexin-beta |