5KR2
Protease PR5-SQV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-12-16 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.890, 62.670, 58.400 |
Unit cell angles | 90.00, 98.59, 90.00 |
Refinement procedure
Resolution | 22.061 - 1.780 |
R-factor | 0.193 |
Rwork | 0.190 |
R-free | 0.23260 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.092 |
Data reduction software | iMOSFLM (7.1.1) |
Data scaling software | Aimless |
Phasing software | PHASER (2.1) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 26.600 |
High resolution limit [Å] | 1.700 |
Number of reflections | 32248 |
<I/σ(I)> | 12 |
Completeness [%] | 92.6 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 300 | Ammonium sulfate |