5KR2
Protease PR5-SQV
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2014-12-16 |
| Detector | RIGAKU |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 50.890, 62.670, 58.400 |
| Unit cell angles | 90.00, 98.59, 90.00 |
Refinement procedure
| Resolution | 22.061 - 1.780 |
| R-factor | 0.193 |
| Rwork | 0.190 |
| R-free | 0.23260 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.092 |
| Data reduction software | iMOSFLM (7.1.1) |
| Data scaling software | Aimless |
| Phasing software | PHASER (2.1) |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 26.600 |
| High resolution limit [Å] | 1.700 |
| Number of reflections | 32248 |
| <I/σ(I)> | 12 |
| Completeness [%] | 92.6 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 300 | Ammonium sulfate |
