5KQY
Protease E35D-DRV
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2015-02-14 |
| Detector | RIGAKU |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 2 21 21 |
| Unit cell lengths | 45.580, 58.170, 86.160 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 17.067 - 1.650 |
| R-factor | 0.1841 |
| Rwork | 0.183 |
| R-free | 0.20240 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.167 |
| Data reduction software | iMOSFLM (7.1.1) |
| Data scaling software | Aimless |
| Phasing software | PHASER (2.1) |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 17.900 |
| High resolution limit [Å] | 1.600 |
| Number of reflections | 28265 |
| <I/σ(I)> | 9.8 |
| Completeness [%] | 99.9 |
| Redundancy | 6.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 300 | sodium chloride |
