5KNG
CRYSTAL STRUCTURE OF ANTI-IL-13 DARPIN 6G9
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-02-06 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9999 |
| Spacegroup name | H 3 |
| Unit cell lengths | 96.080, 96.080, 206.430 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.000 - 1.350 |
| R-factor | 0.17434 |
| Rwork | 0.174 |
| R-free | 0.19676 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2j8s |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.088 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.390 |
| High resolution limit [Å] | 1.350 | 1.350 |
| Rmerge | 0.055 | 0.469 |
| Number of reflections | 156050 | |
| <I/σ(I)> | 15.5 | 3.3 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 5.1 | 5.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 0.4 M NH4H2PO4 |
