5KJV
Crystal structure of Coleus blumei HCT
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-E |
| Synchrotron site | APS |
| Beamline | 24-ID-E |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-11-06 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 1 |
| Unit cell lengths | 37.550, 56.690, 107.840 |
| Unit cell angles | 83.22, 89.65, 72.29 |
Refinement procedure
| Resolution | 50.454 - 1.750 |
| R-factor | 0.1716 |
| Rwork | 0.171 |
| R-free | 0.21120 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.459 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | PHENIX (dev_1839) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 53.600 |
| High resolution limit [Å] | 1.750 |
| Number of reflections | 199588 |
| <I/σ(I)> | 5.8 |
| Completeness [%] | 90.2 |
| Redundancy | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277.15 | 0.1 M Bis-Tris:HCl, 25% PEG 3350, pH 7.5 |
