5KH8

Solution structures of the apo state fluoride riboswitch

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600
2	Bruker	AVANCE III		500

Experiment

experiment id	conditions id	solution id	Experiment type
1	2	1	2D 1H-1H NOESY
10	1	6	2D HCCH COSY
11	1	6	31P spin-echo
12	1	5	31P spin-echo
13	1	6	3D HCCH-TOCSY
14	1	5	3D HCCH-TOCSY
15	1	3	2D 1H-13C HSQC
16	1	5	CH-HCCH spin-echo
17	1	3	2D 1H-15N HSQC
18	1	6	CH-HCCH spin-echo
2	1	2	2D 1H-1H NOESY
3	1	2	2D 1H-1H TOCSY
4	2	3	2D 1H-15N HSQC
5	2	3	2D 1H-13C HSQC
6	1	5	2D 1H-13C HSQC
7	1	4	2D 1H-13C HSQC
8	1	5	2D HCCH COSY
9	1	6	2D 1H-13C HSQC

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.4	ambient	303
2	6.4	ambient	283

Conformers

Conformers Calculated Total Number
Conformers Submitted Total Number	20