5KGR
Spin-Labeled T4 Lysozyme Construct I9V1/V131V1 (30 days)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-19 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 60.031, 60.031, 95.509 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.169 - 1.473 |
R-factor | 0.1673 |
Rwork | 0.166 |
R-free | 0.18900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c6t |
RMSD bond length | 0.017 |
RMSD bond angle | 0.805 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.170 | |
High resolution limit [Å] | 1.470 | 1.470 |
Rmerge | 0.049 | |
Number of reflections | 34344 | |
<I/σ(I)> | 8.86 | |
Completeness [%] | 100.0 | |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2 M sodium/potassium phosphate, 150 mM sodium chloride, 100 mM 1,2-hexanediol, 3% 2-propanol |