5KC8
Crystal structure of the amino-terminal domain (ATD) of iGluR Delta-2 (GluD2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-27 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00000 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 45.100, 79.160, 246.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.871 - 1.751 |
R-factor | 0.1907 |
Rwork | 0.189 |
R-free | 0.21840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wjw |
RMSD bond length | 0.008 |
RMSD bond angle | 0.917 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1772) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.030 | 1.800 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.078 | 1.314 |
Number of reflections | 44958 | |
<I/σ(I)> | 24.2 | 2.2 |
Completeness [%] | 99.6 | 98.3 |
Redundancy | 15.3 | 9.5 |
CC(1/2) | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% (w/v) polyethylene glycol 1000, 0.2 M calcium Acetate, 0.1 M imidazole pH 8.0 and 0.4 M NDSB-221 (non-detergent sulfobetaine 221) |