5KC4
Structure of TmRibU, orthorhombic crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-17 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.008 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.769, 80.784, 118.028 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.916 - 3.400 |
R-factor | 0.2501 |
Rwork | 0.249 |
R-free | 0.26960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5kc0 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.752 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.916 | 3.480 |
High resolution limit [Å] | 3.400 | 3.400 |
Number of reflections | 8513 | |
<I/σ(I)> | 24.6 | |
Completeness [%] | 94.5 | |
Redundancy | 14.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 289 | 100 mM Tris, pH 8.5, 30% PEG400, 100 mM NaCl, 0.5% NG, and 1% hexanediol |