5KAZ
Human SH2D1B structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-03-09 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 66.983, 66.983, 105.155 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.191 - 1.700 |
R-factor | 0.1907 |
Rwork | 0.189 |
R-free | 0.21430 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.209 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 31.054 |
High resolution limit [Å] | 1.700 |
Number of reflections | 13571 |
<I/σ(I)> | 33.9 |
Completeness [%] | 98.8 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M Na-Citrate pH 5.5, 24% PEG 4000, 50 mM (NH)2SO4 |